去感热注射液指纹图谱进样方式的研究  

Study on the Fingerprint Precedures of Quganre Injection Sampling

作　　者：易秋艳[1] 黄瑛[1] 刘仲义[1] 

机构地区：[1]四川省食品药品检验所,四川成都610036

出　　处：《西南军医》2008年第6期30-31,共2页Journal of Military Surgeon in Southwest China

摘　　要：目的建立去感热注射液挥发性成分指纹图谱的进样方式。方法采用直接进样、固相微萃取、有机溶剂提取、吹扫捕集和顶空进样等进样方式进行比较。结果选定顶空进样为指纹图谱研究的进样方式。结论本方法为去感热注射液的挥发性成分的指纹图谱研究提供了可靠的进样方式。Objective To set up the most suitable sampling injection mode for the fingerprint of the volatile components in Quganre Injection. Methods The techniques of direct injection, solid-phase microextraction, organic solvbent extraction, purge-trap sampling and headspace sampling were applied, their effects in fingerpring were compared. Results Headspace sampling was chosen for finger- print study. Conclusion Headspace sampling is reliable in studying the fingerprint of volatile components in Quganre Injection.

关 键 词：去感热注射液 气相色谱 指纹图谱 

分 类 号：R222.18[医药卫生—中医基础理论]