3,6-二氯荧烷的新合成方法及其光谱鉴定  

An accidental synthesis of 3,6-dichlorofluorane and its spectroscopic identification

作　　者：王流芳[1] 任艳平[1] 袁希召 何凤英[2] 王淇 

机构地区：[1]兰州大学化学系 [2]甘肃省分析测试中心 [3]兰州化学物理研究所

出　　处：《化学试剂》1990年第6期341-343,326,共4页Chemical Reagents

摘　　要：用新的方法合成了题目化合物。通过元素分析、IR、EIMS、~1HNMR 验证了分子组成及结构,并对其生成机理进行了探讨。The title compound I was synthesized with a new method accidentally.Its composition andstructure were confirmed by elementary analysisand IR,NMR and MS spectra.In this paper theprobable mechanism of its formation is discussed.I is well known as a highly sensitive fluo-rescent dyestuff for biocells.We have found thatit also has strong inhibitory and killing effecton cultivated murine leukemia cell(L_(?))andhuman stomach cancer cell(SGC-7901),the re-sult will be reported later.

关 键 词：二氯荧烷 合成 光谱鉴定 

分 类 号：R914.5[医药卫生—药物化学]