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作 者:张小曼[1]
出 处:《化学工程师》2008年第12期60-62,共3页Chemical Engineer
摘 要:利用Ce(SO4)2.4H2O作为催化剂合成了己酸异戊酯,其最佳反应条件为:催化剂用量1.0g,醇酸摩尔比1.8∶1.0,带水剂(环己烷)15mL,反应时间2.0h,酯化率可达97.2%。该催化剂易分离回收,可重复使用。Isoamyl hexanoate has been synthesized by using ceric sulfate as catalyst. The optimized condition are follow: the weight of catalyst is 1.0g, the mole ratio of alcohol to acid is 1.8:1.0, the reaction time is 2. Oh and the taking water reagent (cyclobexane) was 15mL ,The esterification yield is 97.2%. The catalyst could be i- solated from other matters and repetition use.
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