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机构地区:[1]宁波市产品质量监督检验研究院,浙江宁波315041 [2]武汉大学化学与分子科学学院,湖北武汉430072
出 处:《中国塑料》2010年第7期92-97,共6页China Plastics
基 金:国家质检总局科技计划项目(2007QK153);宁波市自然科学基金项目(2009A610182)
摘 要:将市售的微波爆米花包装袋用微波感受材料浸入模拟食品玉米油中,在模拟微波条件下加热提取非挥发性紫外可吸收物质。迁移进玉米油中的非挥发性紫外可吸收物质经正己烷-乙腈萃取、浓缩、N,N-二甲基乙酰胺定容至2 mL后,以高效液相色谱分离并定量。结果表明,4个样品的迁移量平均值分别为93.3、134.1、38.4和11.8μg/in2,仅1个样品的迁移量符合美国食品药品监督管理局(FDA)规定的≤20μg/in2的限量标准。In this paper, microwave susceptors in the microwave popcorn bags were immergecl into corn oil. When the system was heated in a microwave oven, some nonvolatile ultraviolet absorbing species were migrated into the corn oil. Such nonvolatile ultraviolet absorbing species were then extracted by hexane-acetonitrile. With water bath and a gentle nitrogen stream, the extract was dried and concentrated, and subsequently kept as a solution of dimethylacetamide of 2 mL. The extract was finally separated with a high performance liquid chromatography and weighed. The weights of the extracts for four samples were 93. 3, 134. 1, 38. 4 and 11.8μg/in2, respectively. Only one of these samples was below the FDA's safety limit standard of 20/μg/in2.
关 键 词:微波爆米花 微波感受材料 非挥发性紫外可吸收物 迁移
分 类 号:TS206.4[轻工技术与工程—食品科学]
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