低温溶液法合成一维ZnO纳米管  

Synthesis of One Dimensional ZnO Nanotubes by Low Temperature Solution Method

作　　者：宫丽红[1,2] 叶彩[2] 安茂忠[1] 

机构地区：[1]哈尔滨工业大学化工学院,黑龙江哈尔滨150001 [2]哈尔滨师范大学化学化工学院,黑龙江哈尔滨150025

出　　处：《合成化学》2010年第4期503-506,共4页Chinese Journal of Synthetic Chemistry

基　　金：黑龙江省教育厅科技研究项目(11531236)

摘　　要：以硝酸锌为锌源,25%氨水为碱液,在pH10的条件下,于75℃反应11 h合成了一维ZnO纳米管。用XRD,SEM,Raman和可见分光光度计对其形貌、结构和光学性能进行了研究。结果表明,ZnO纳米管为规则的六棱柱,平均直径100 nm,长度达数微米。One-dimensional ZnO nanotubes were synthesized by low temperature solution method using zinc nitrate as the zine source and 25% ammonia as the alkali liquor at pH 10 and 75 ℃ for 11 h.The structure,morphology and optical property were investigated by XRD,SEM,Raman and visible spectrophotometer.The results showed that ZnO exhibited a hexahedron shape with an average diameter of 100 nm and the length of several micrometers.

关 键 词：纳米材料 ZNO 低温溶液法 合成 

分 类 号：O614.24[理学—无机化学]