粉檀麝香的示波极谱法测定  

DETERMINATION OF PHANTOLIDE BY SINGLESWEEP POLAROGRAPHY

作　　者：张志红[1] 刘壮[1] 袁荣根 张辉 

机构地区：[1]北京石油化工学院化工系,102600

出　　处：《精细石油化工》1999年第2期55-57,共3页Speciality Petrochemicals

摘　　要：建立了一种粉檀麝香的单扫描极谱的测定方法。研究发现 :在 0 .1 2 mol/ L的 H3PO4甲醇水溶液中 ,粉檀麝香有一个灵敏的极谱还原波 ,峰电位为 -0 .32 V( SCE) ,其一阶导数波高与粉檀麝香的浓度在 4 .0× 1 0 - 5～ 4 .0× 1 0 - 4 mol/ L之间呈线性关系 ,它可以用于粉檀麝香的测定。A method for the determination of phantolide by using singlesweep polargraphy was established. In 0.12 mol/L H 3PO 4 methanolwater mixture solution, phantolide showed a polarographic reduction wave. Its peak potential was -0.32V(SCE). The frist order deviation peak height was linear with concentration of phantolide in the range in 4.0×10 -5 ～4.0×10 -4 mol/L. So this method could be used to indirect determination phantolide.

关 键 词：粉檀麝香 单扫描极谱 极谱法 香料 动物香料 

分 类 号：TQ654.1[化学工程—精细化工] TQ651.2