高效液相色谱法测定肉制品中硫酸阿托品含量  

Determination of atropine sulfate in meat by HPLC

作　　者：李长缨[1] 李东方[2] 于波[2] 

机构地区：[1]重庆大学医院,重庆400045 [2]沈阳市疾病预防控制中心,沈阳110031

出　　处：《中国卫生检验杂志》2011年第5期1090-1091,共2页Chinese Journal of Health Laboratory Technology

摘　　要：目的：建立肉制品中硫酸阿托品的测定方法。方法：采用超声波提取工艺,以高效液相色谱法（HPLC）法对肉制品中的硫酸阿托品含量进行测定。结果：本法的精密度在3.9%-4.5%之间,回收率在81.3%-88.9%。结论：本法操作较为简便,具有较好的精密度和准确度,适合于肉制品中的硫酸阿托品含量测定。Objective：To develop a method for the determination of atropine sulfate in meat.Methods： Ultrasonic technique was applied to extract atropine sulfate and HPLC method was used to determine them.Results： The RSD were in the range of 3.9%-4.5% and the recoveries were in the range of 81.3%-88.9%.Conclusion： The developed method is simple,sensitive,accurate,and reliable for the determination of atropine sulfate in meat.

关 键 词：肉制品 硫酸阿托品 超声波提取 高效液相色谱 

分 类 号：O657.72[理学—分析化学]