香芹类香料的研制  

Preparation of Celery Spices

作　　者：纪文华[1] 高乾善[1] 

机构地区：[1]山东省分析测试中心,山东济南250014

出　　处：《山东科学》2011年第3期83-86,共4页Shandong Science

摘　　要：为制备香芹类香料,以香芹酮为原料,采用锌-醇还原、硼氢化钠还原、乙酸酐酯化等方法合成了二氢香芹酮、二氢香芹醇、乙酸二氢香芹酯。重点研究了锌粉在不同溶剂中的还原效果。目标化合物的结构利用核磁共振、质谱做了确证,该合成路线操作简便,收率高(高于80%),成本低,对工业化生产有一定参考价值。This paper addressed preparation methods of dihydrocarvone,dihydrocarveol and dihydrocarvyl acetate with carvone as raw material and such steps as reduction,esterification,especially the Zn-ROH reduction.We employed NMR and ESI-MS to determine the structures of these objective compounds.This synthesis process has such positives as low cost and high recovery rate（more than 80%）,and has some references to industrial production.

关 键 词：香芹酮 香料 合成 

分 类 号：TQ655[化学工程—精细化工]