A New Route for Identification of Precipitates on Austenite Grain Boundary in an Nb-V-Ti Microalloyed Steel  

作　　者：SHA Qing-yun HUANG Guo-jian GUAN Ju MA Xiao-jun LI Da-hang 

机构地区：[1]Technology Center, Angang Steel Company Limited, Anshan 114009, Liaoning, China

出　　处：《Journal of Iron and Steel Research International》2011年第8期53-57,共5页

摘　　要：The precipitates on austenite grain boundaries in an Nb-V-Ti microalloyed steel have been investigated by transmission electron microscope （TEM） examination of carbon extraction replica. The replica was prepared from specimen etched with saturated picric solution rather than Nital which is conventionally used. Then particles on both grain boundaries and triple point of grain [aoundaries were clearly observed and identified as （Nb,Ti）（C, N） parti- cles. In case of conventional way, it is difficult to determine the location of particles with respect to austenite grain boundaries. The number of particles observed in new way developed was greatly reduced compared with that found in replica prepared by the conventional way, which may be caused by the dissolution of partial precipitates during the etching with longer time and at higher temperature involved in new way. Despite this, the new way developed pro- vides an effective way to determine the precipitate particles on austenite urain boundaries_The precipitates on austenite grain boundaries in an Nb-V-Ti microalloyed steel have been investigated by transmission electron microscope （TEM） examination of carbon extraction replica. The replica was prepared from specimen etched with saturated picric solution rather than Nital which is conventionally used. Then particles on both grain boundaries and triple point of grain [aoundaries were clearly observed and identified as （Nb,Ti）（C, N） parti- cles. In case of conventional way, it is difficult to determine the location of particles with respect to austenite grain boundaries. The number of particles observed in new way developed was greatly reduced compared with that found in replica prepared by the conventional way, which may be caused by the dissolution of partial precipitates during the etching with longer time and at higher temperature involved in new way. Despite this, the new way developed pro- vides an effective way to determine the precipitate particles on austenite urain boundaries_

关 键 词：PRECIPITATE austenite grain boundary REPLICA ETCH 

分 类 号：TG142.33[一般工业技术—材料科学与工程] TG142.1[金属学及工艺—金属材料]