香粉叶挥发性成分的提取和分析  

Extraction and Analysis of Volatile Constituents from Lindera Pulcherrima(Wall.)

作　　者：黄品鲜[1] 赖芳[2] 周永红[2] 刘雄民[2] 

机构地区：[1]广西大学科技处,南宁530004 [2]广西大学化学化工学院,南宁530004

出　　处：《应用化学》2012年第3期311-315,共5页Chinese Journal of Applied Chemistry

基　　金：广西省自然科学基金项目(0832002);广西省教育厅科研项目(200807MS149)

摘　　要：采用水蒸汽蒸馏法提取香粉叶的挥发组分,用乙醚萃取蒸馏溶液的挥发性成份,利用气相色谱-质谱联用仪分别定性定量分析了它们的化学成分。结果表明,挥发油的提取率为0.75%(质量百分数,以下同),主要成分有:1,8-桉叶素28.94%、α-甲基香豆酮15.75%、4-松油醇5.13%、α-松油醇11.22%、2-羟基肉桂酸7.97%、愈创木醇2.87%。水层乙醚萃取物得率为0.25%,主要成分有:2-甲基苯并呋喃8.47%、2H-1-苯并吡喃-2-酮24.13%、2H-1-苯并吡喃-3-醇-3,4-二氢乙酸酯18.07%、p-羟甲苯基缩水甘油醚2.09%、1-苯基苯乙基-3,3-二乙酯4.50%、丙三醇二乙酸酯17.19%、乙酸金合欢酯11.80%。The volatile constituents of Lindera Pulcherrima（Wall. ） were extracted by steam distillation. The chemical constituents of essential oil have been analyzed by GC-MS. The results show that the extractive yield of essential oil is 0. 75%, the compounds of essential oil are 28. 94% eucalyptol, 15.75% a-methlybenzofuran, 5. 13% 4-terpinenol, 11.22% a-terpineol, 7.97% 2-hydroxycinnamic acid, 2.87% guaiol, and the extractive yield of substance from water is 0. 25%, which consists of 8.47% 2-methylbenzofuran, 24. 13% 2H-1-benzopyran-2-one, 18.07% 2H-l-benzopyran-3-ol, 3,4-dihydro-, acetate, 2.09% p-gresyl glycidyl ether, 4. 50% 1-phenylpropene-3,3-diol diacetate, 17. 19% glycerol dicetate and 11.80% farnesyl acetate.

关 键 词：香粉叶 挥发性成分 提取 GC-MS 

分 类 号：O629.6[理学—有机化学]