气相色谱法测定儿腹康贴剂中丁香酚的含量  

DETERMINATION OF CONTENT OF SYINGIC PHENOL EN ERFUKANG BY GAS CHROMATOGRAPHY

作　　者：李青[1] 方赤光[1] 于峰[1] 张冠英[1] 王隶书[2] 孙云 

机构地区：[1]吉林省卫生防疫站,长春130021 [2]吉林省中医中药研究院,长春130021 [3]吉林省监狱管理局中心医院,长春130052

出　　处：《化学分析计量》2000年第2期20-21,共2页Chemical Analysis And Meterage

摘　　要：采用气相色谱法(15％聚乙二醇20M+10％阿匹松柱)测定儿腹康贴剂中丁香酚的含量,线性范围为0.1～1.0g/L,以正十七烷为内标,重复性好,加标回收率较高。The GC method for determination of content of syingic phenol in erfukang sticking was established.The conditions for determination were; 15% polyethylene glycol-20 M + 10% Apiezon on 100 ~ 120 mesh chromosorb WAW-DMCS packed in a 1 m×3 mm i d.Both FID detector and injector port at 230℃.Heptadecane was used as internal standard,The response was linear between 0.1 g/L and 1.0 g/L.This method is proved to be highly sensitive,good reproducible and satisfactory.

关 键 词：儿腹康贴剂 气相色谱法 丁香酚 中药 止泻药 

分 类 号：R286.53[医药卫生—中药学] R284.1[医药卫生—中医学]