高效液相色谱法测定地表灰尘中的16种多环芳烃  

The Determination for 16 Polycyclic Aromatic Hydrocarbons in Surface Dust by High Performance Liquid Chromatography

作　　者：王娅[1] 方志青[1] 林野[2] 杨成[1] 严敏[1] 贺华中[1] 王雅洁[1] 

机构地区：[1]贵州民族学院化学与环境科学学院,贵州贵阳550025 [2]贵州省疾病预防控制中心,贵州贵阳550004

出　　处：《江西师范大学学报（自然科学版）》2012年第3期313-316,共4页Journal of Jiangxi Normal University(Natural Science Edition)

基　　金：贵州省科学技术基金([2009]2037号)资助项目

摘　　要：用高效液相色谱分析方法测定了地表灰尘中16种多环芳烃.样品经超声提取、硅胶萃取柱净化后,用液相色谱测定.优化了试验条件,16种多环芳烃的检出限为0.08~4.65μg/kg,方法线性关系良好,基质加标回收率为77.6%~113.7%,相对标准偏差为1.26%~7.32%.The determination method of 16 PAHs in surface dust was studied by HPLC, the samples were pretreated by ultrasonic extraction with dichlormethane and acetone as solvent, silica purification, hexane and dichlormethane washing. The results demonstrated the detection limits of method for 16 PAHs were from 0.08 to 4.65 μg/kg with good linearity, the recoveries of standard addition ranged from 77.6% to 113.7%, relative standard deviation varied between 1.26% and 7.32%.

关 键 词：多环芳烃 地表灰尘 固相萃取 高效液相色谱法 

分 类 号：O626.4[理学—有机化学]