高效液相色谱法检测皮革中3种防腐剂  

Determination of Three Preservatives in Leather by High Performance Liquid Chromatography Method

作　　者：毛树禄 尹洪雷 连小彬 张元金 李小娅 

机构地区：[1]泉州出入境检验检疫局国家鞋类检测中心,福建晋江362200

出　　处：《中国皮革》2013年第1期30-33,共4页China Leather

基　　金：国家质检总局科研项目(2010IK100)资助

摘　　要：研究并优化了皮革中3种防腐剂的高效液相色谱(HPLC-DAD)检测方法。皮革样品经乙腈超声提取20min,滤液滤膜过滤后进行HPLC-DAD测定。流动相为乙腈/水,柱温40℃,DAD波长为225nm。当标样的浓度为0.5～10mg/L时,线性相关系数R2≥0.99,最高检出限5mg/kg,加标回收率在85%～106%之间。Determination of three preservatives in leather was developed by HPLC - DAD. Leather sample was treated for 20 min in acetonitrile by ultrasonic assisted extraction, The solution was then filtered through film. The mobile phase is acetonitrile and water. The column temperature is 40℃ and the detection wavelength is 225nm. The linear correlation coefficient is bigger than0.99 at the concentration of 0.5 - 10mg/L. The highest detection limit is 5mg/kg. The recoveries are at the range of 85% ~ 106%.

关 键 词：皮革 防腐剂 高效液相色谱 

分 类 号：TS57[轻工技术与工程—皮革化学与工程]