Clevenger法提取草果精油的化学组成及清除NaNO_2能力  被引量:10

Chemical Components and NaNO_2 Scavenging Ability of Amomum Tsao-ko Essential Oil Extacted by Clevenger Method

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作  者:陆占国[1] 孟大威[1] 李伟[1] 王鹏君[2] 任慧峰[3] 

机构地区:[1]哈尔滨商业大学食品工程学院省高校食品科学与工程重点实验室,哈尔滨150076 [2]燕山大学环境与化学工程学院,秦皇岛066004 [3]东京海洋大学海洋环境学科

出  处:《天然产物研究与开发》2013年第2期207-211,共5页Natural Product Research and Development

摘  要:采用Clevenger法提取草果精油,以1.87%的平均得油率获得精油,用GC-MS联机对精油进行了成分分析,检测出38种成分,解析鉴定了占总成分98.393%的32个成分。主要成分1,8-桉树脑占40.891%(相对含量,以下同),α-水芹烯9.769%,2-异丙基苯甲醛6.988%。测定精油清除NaNO2能力结果可知:当精油用量为0.15~0.45 mL时,清除率为68.22%~81.40%,大于对照物Vc(57.12%~78.16%)和BHT(14.64%~18.66%)(精油和对照物浓度10 mg/mL)。The essential oil was obtained in 1.87% y/eld from Amwwan tsao-ko by clevenger method. The chemical components of the essential oil were analyzed by GC-MS. 38 components were detected and 32 compounds which occupied 98. 393% (relative content) of the total constituents were identified. The main components were 1,8-cinecl (40. 891% ) ,a-phel-landrene (9.769%) and 2-isopropylbenzaldehyde (6. 988% ). The ability of scavenging sodium nitrite of essential oil was investigated. The results showed that the essential oil had considerable effect of scavenging NaNO2 ,the scavenging rate were 68.22%-81.40% when 0.15-0.35 mL of the oil was used. It was higher than Vc (57. 12%-78. i6%) and BHT (14.64%-18.66% ) which were used as controls (conc/entraetion of essential oil, Vc and BHT are 10 mg/mL).

关 键 词:草果 精油 气相色谱-质谱 NaNO2 

分 类 号:TQ656.1[化学工程—精细化工]

 

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