长白山复序橐吾花挥发油化学成分的分析  

Components analysis of volatile oil from flower of Ligularia jaluens in Changbai Mountains

作　　者：朱梅[1,2] 刘洪章[1] 董然[1] 刘淑英[1] 

机构地区：[1]吉林农业大学生命科学学院,长春130118 [2]北华大学化学与生物学院,吉林吉林132013

出　　处：《东北农业大学学报》2013年第4期101-105,共5页Journal of Northeast Agricultural University

基　　金：吉林省科技发展计划项目(20100254)

摘　　要：以复序橐吾花为试验材料,采用水蒸气蒸馏法对挥发油进行提取,通过GC-MS联用技术对其挥发性成分进行分析鉴定,利用峰面积归一化法计算各化合物的相对质量分数。结果表明,从复序橐吾花挥发油中分离得到49个色谱峰,共鉴定出39个化合物,占挥发油总量的94.80%,主要化学成分为4-蒈烯(26.534%)、D-柠檬烯(13.325%)、1-甲苯基-乙酮(7.231%)、α,α,4-三甲基-3-环己烯-1-甲醇(6.379%)、β-水芹烯(5.700%)。In the experiment the essential oils of the herb were extracted with steam distillation and chemical components were identified by GC-MS. The components were quantitatively determined with the normalization method and identified results showed by columns area. As a result, 49 peaks were detected, among which 39 compounds had been identified, which made up 94.80% of the total volatile oil, in which the main chemical components of L. jaluensis are 4-Carene（26.534%）, D-Limonene （13.325%） and Ethanone, 1-（methylphenyl） （7.231%）, 3-Cyclohexene-l-methanol,.alpha.,.alpha.4-trime- thy （6.379%）, beta.-Phellandren（5.700%）.

关 键 词：复序橐吾 花 挥发油 气相色谱-质谱联用 

分 类 号：R284[医药卫生—中药学]