超声波强化溶剂法连续提取烟草中油溶性及水溶性成分研究  

Study on the Continuous Ultrasonic-assisted Solvent Extraction Technology of Petroleum Ether Extracts and Water Extracts from Tobacco

作　　者：张旗[1,2] 黄龙[1] 高志农[2] 黄明[1] 姚元军[1] 

机构地区：[1]湖北中烟工业有限责任公司技术中心,武汉430040 [2]武汉大学化学与分子科学学院,武汉430072

出　　处：《食品工业》2013年第12期155-159,共5页The Food Industry

摘　　要：采用超声波强化溶剂萃取法对烟草原料进行了石油醚-水两步萃取研究,在单因素试验的基础上,利用正交试验方法对每步的超声萃取工艺参数进行了优化。结果表明,最优工艺参数为:第一步石油醚提取温度50℃,提取时间60 min,提取料液质量比1︰10,超声功率200 W;第二步水提取温度50℃,提取时间60 min,提取料液质量比1︰15,超声功率200 W。在此条件下石油醚提取及水提取物平均得率分别达到3.32%和56.14%,均明显高于传统加热提取方式。The petroleum ether-water twice extraction of tobacco using ultrasonic-assisted method was studied. On the basis of single factor experiments, the key parameters for ultrasonic-assisted solvent extraction were analyzed and optimized using orthogonal experiment design. The results indicated that the optimal values ofpararneters for petroleum ether extraction were as follows： extraction temperature 50 ℃, ultrasonic treatment time 60 rain, material-solvent ratio 1 ： 10, ultrasonic power 200 W, and the optimal values of parameters for water extraction were as follows： extraction temperature 50 ℃, ultrasonic treatment time 60rain, material-solvent ratio 1 ： 15, ultrasonic power 200 W. Under such conditions, the average yield of optimal petroleum ether extracts and water extracts from tobacco reached 3.32% and 56.14%, respectively, which were significantly higher than the yield of traditional heat extraction.

关 键 词：超声波强化 连续提取 烟草 石油醚提取物 水提取物 

分 类 号：TS44[农业科学—烟草工业]