毛细管柱气相色谱内标法测定岩桂叶精油中黄樟油素含量  

Determination of Safrole Content in the Essential Oil of Cinnamomum petrophilum N.Chao Leaves by Capillary Column Gas Chromatography with Internal Standard Method

作　　者：尹礼国[1,2,3] 徐洲[1,2,3] 张超[1,2] 魏琴[1,2] 

机构地区：[1]宜宾学院发酵资源与应用四川省高校重点实验室,四川宜宾644007 [2]宜宾学院生命科学与食品工程学院,四川宜宾644007 [3]宜宾学院食品科学与工程研究所,四川宜宾644007

出　　处：《生物质化学工程》2014年第5期11-14,共4页Biomass Chemical Engineering

基　　金：四川省科技厅项目(项目编号2009JY0057)

摘　　要：为了快速准确测定岩桂叶精油中黄樟油素含量，建立了毛细管柱气相色谱内标法，对岩桂叶精油中黄樟油素含量进行检测，结果表明，岩桂叶精油中黄樟油素GC含量为92.9%~94.3%。该方法的相对标准偏差小于0.5%，检测时间为8 min，检测精密度和准确度高，时间短，可快速测定黄樟油素含量。In order to determine safrole content in the essential oil of Cinnamomum petrophilum N. Chao leaves rapidly,the capillary column gas chromatography with internal standard method was set up. The safrole contents of the essential oils were 92. 9% to 94. 3%. The relative standard deviation（ RSD）of the detection method was less than 0. 5%,and the detection time was 8 min. The method was rapid,accurate and precise.

关 键 词：岩桂 精油 气相色谱 内标法 黄樟油素 

分 类 号：O657.71[理学—分析化学] TQ654.2[理学—化学]