微波消解塞曼石墨炉原子吸收法测定大米中微量镍  

A Determination of Trace Nickel in Rice by Microwave Digestion And Graphite Furnace Atomic Absorption Spectrometry

作　　者：袁友明[1] 姚晶晶[1] 路磊[1] 陶宁丽[1] 

机构地区：[1]农业部食品质量监督检验测试中心,湖北武汉430064

出　　处：《绿色科技》2014年第10期221-222,共2页Journal of Green Science and Technology

摘　　要：利用微波消解技术处理样品,用塞曼石墨炉原子吸收法测定了大米中的镍,该方法具有简便、快速、结果准确可靠的优点。测定结果表明：镍的浓度在0~25μg/L范围线性良好,相关系数0.9991,镍的加标回收率为97.3%~104.2%;测定结果的相对标准偏差为1.9%,检出限为0.152μg/L。This article adopts microwave digestion technology to process the sample absorption spectrometry to determine the trace Nickel in rice. The proposed method accurate. The test results show that the linear range of Nickel is 0--25μg/L with a The adding standard recovery is in the range of 97. 3%- 104, 2%, the RSD and uses graphite furnace atomic is proved to be rapid, simple and correlation coefficient of 0. 9991. is 1. 9 %, and detection limitis 0. 152μg/L.

关 键 词：大米 镍 微波消解 塞曼石墨炉原子吸收 

分 类 号：TS212[轻工技术与工程—粮食、油脂及植物蛋白工程]