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作 者:孙海林[1] 张雅琼[1] 谢小燕[1] 车彦云[1]
机构地区:[1]云南中医学院,云南昆明650500
出 处:《中药材》2014年第11期2019-2021,共3页Journal of Chinese Medicinal Materials
摘 要:目的:研究睡莲科芡属植物芡Euryale ferox Salisb.的成熟种仁芡实的化学成分。方法:对芡实95%乙醇提取物的石油醚和乙酸乙酯部位采用硅胶柱色谱、Sephadex LH-20柱色谱等方法分离纯化;根据理化性质和波谱数据鉴定化合物结构。结果:从芡实中分离并鉴定了7个化合物,分别为:原儿茶酸(1)、没食子酸(2)、没食子酸乙酯(3)、5,7-二羟基色原酮(4)、β-谷甾醇(5)、胡萝卜苷(6)、5,7-二羟基-6,4'-二甲氧基黄酮(7)。结论:以上化合物均为首次从该植物中分离得到。Objective: To study the chemical constituents from the seeds of Euryale ferox. Methods: The chemical constituents were isolated by silica gel column,Sephadex LH-20 and their structures were identified by physico-chemical and spectral analysis. Results:Seven compounds were purified from the 95% ethanol extract. These constituents were elucidated as protocatechuic acid( 1),gallic acid( 2),gallic acid ethyl ester( 3),5,7-dihydroxychromone( 4),β-sitosterol( 5),daucosterol( 6),and 5,7-dihydroxy-6,4'-dimethoxyflavone( 7),respectively. Conclusion: All compounds are isolated from this plant for the first time.
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