水热法制备镉功能配合物材料研究型综合实验  

Research-oriented Comprehensive Chemical Experiment on Synthesis of Cadmium Functional Complex Materials by Hydrothermal Method

作　　者：彭艳芬[1] 刘天宝[1] 

机构地区：[1]池州学院化学与材料工程学院,安徽池州247000

出　　处：《蚌埠学院学报》2017年第6期56-58,83,共4页Journal of Bengbu University

基　　金：安徽省自然科学基金重点项目(KJ2016A512);安徽省高校优秀青年人才支持计划重点项目(gxyq ZD2016372);安徽省质量工程MOOC示范项目(2015MOOC092);池州学院教研项目(2016XJYXM71)

摘　　要：设计一个研究型综合实验,以1,2-二(4H-1,2,4-三唑)乙烷和1,2,3-联苯三甲酸为配体,与Cd(NO3)2通过水热反应法合成一个具有荧光性质的配合物材料。该实验项目集有机合成实验、无机合成实验和仪器分析实验于一体,可以培养学生的实践动手能力、科研创新能力以及综合运用知识的能力,具有较强的可操作性和实用性,可作为基础化学研究型综合实验或开放性实验开设。A research-oriented comprehensive chemistry experiment was introduced in this paper,and a fluorescent complex material was synthesized by hydrothermal reaction with 1,2,3-benzenetricarboxylic acid,1,2-bis(4 H-1,2,4-triazole) ethane and Cd(NO3)2.The organic synthesis experiment,the inorganic synthesis experiment and the instrumental analysis experiment were unified into this experiment project.Students practical ability,scientific research innovation ability and comprehensive ability of using knowledge can be improved.It has good operability and practicability,and can be established as a research-oriented comprehensive chemical experiment or open experiment.

关 键 词：1 2-二(4H-1 2 4-三唑)乙烷 水热反应 荧光 综合实验 

分 类 号：G642[文化科学—高等教育学] O641.4-4[文化科学—教育学]