蜂胶中四环素族药物残留检测方法研究  

Researches of Detection for Tetracycline Drugs in Propolis

作　　者：朱文君[1] 张晓燕[1] 吴斌[1] 沈崇钰[1] 丁涛[1] 陈惠兰[1] 

机构地区：[1]江苏出入境检验检疫局动植物与食品检测中心,江苏南京210001

出　　处：《食品研究与开发》2016年第3期135-138,共4页Food Research and Development

基　　金：国家质检总局科研基金项目(2012IK167)

摘　　要：蜂产品中四环素类药物的检测技术日趋成熟,蜂胶作为蜂产品的重要组成部分,其抗生素的检测方法有待进一步的研究和发展。通过分析比较提取液、内标的选择对试验结果的影响,确定试验方法的线性范围和定量限,建立的高效液相-质谱联用法,回收率在74.1%到118.8%之间,精密度在15%以下,能够满足蜂胶产品中四环素药物残留的日常检测。The detection technology of tetracycline drugs in bee products has become mature increasingly. As an important part of bee products, the analytical method in propolis needs to be developed and researched. In this article, we choose different extract and internal standard, the experimental results are different. A linear range and quantitative restrictions were determined by the experiment. The recovery rate was between 74.1 % to118.8 %, the precision of under 15 %.By high performance liquid chromalogphy-tandem mass spechomethy,the detection of tetracycline drugs residues can be satisfied in propolis.

关 键 词：蜂胶 四环素族药物 液相色谱质谱联用 

分 类 号：TS207.53[轻工技术与工程—食品科学]