线性离子阱静电场轨道阱高分辨组合质谱在农药残留快速检测中的应用  

Application of LTQ-Orbitrap Mass Spectrometry Techniques in Pesticide Residue Detection

作　　者：李卫岗[1] 熊岑[2] 郭宗宁 刘秋实[2] 张协光[2] 

机构地区：[1]珠海出入境检验检疫局技术中心,广东珠海519000 [2]深圳市计量质量检测研究院,广东深圳518131 [3]东莞检验检疫局,广东东莞523072

出　　处：《广东化工》2016年第18期161-163,154,共4页Guangdong Chemical Industry

基　　金：珠海出入境检验检疫局科技计划项目(ZH2013-6);深圳市计量质量检测研究院项目(2013-YIA06)

摘　　要：静电场轨道阱(Orbitrap)质谱技术以其优越的高分辨率和高精确质量数的特性,可实现目标物的同分异构体和结构类似物的鉴定以及未知物的筛查和确证。本研究采用线性离子阱静电场轨道阱高分辨组合质谱技术(LTQ-Orbitrap),并采用Qu ECh ERS前处理方法对样品进行提取和净化,建立茶叶和粮食中农药残留的快速筛查确证方法。The Orbitrap Mass Spectrometry Techniques with the high resolving power and mass accuracy can reliably identify the isomeride and structural analogues of target substance, as well as the unknown cornpound. The LTQ-Orbitrap technique, by using the QuEChERS sample preparation for sample extraction and puritication, was used to establish a last screening and confirmation method for pesticide residue detection in tea and cereal samples.

关 键 词：静电场轨道阱质谱 高分辨质谱 农药残留检测 

分 类 号：TQ[化学工程]