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作 者:毛法明
出 处:《染料与染色》2016年第6期5-6,22,共3页Dyestuffs and Coloration
摘 要:对硝基苯胺邻磺酸重氮盐与N-甲基γ酸偶合得单偶氮染料Ⅱ,再经还原,与三聚氯氰一缩,与牛磺酸二缩,与二乙醇胺三缩,最后经盐析,过膜后得墨水红原染料溶液。A monoazo dye was synthesized from 2-amino-5-nitrobenzenesulphonic acid diazonium salt and 4-hydroxy- 6-( methyla mino) naphthalene-2-sulfonic acid by coupling reaction,the dye was reduced by Na2 S,and reacted with cyanuric chloride by firstcondensation; then,reacted with taurine by second-condensation,and reacted with diethanolamine by third-condensation; at last,an inkjet red was obtained by salting-out and membrane filtering.
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