藏药如意珍宝丸的鉴别和含量测定  

QUALITY CONTROL OF RUYI ZHENBAO PILLS

作　　者：王曙[1] 程世琼[2] 蒲怀琼[3] 吴静[1] 达番琼[1] 宋淼[1] 

机构地区：[1]四川大学华西药学院,四川成都610041 [2]四川省药品检验所,四川成都610036 [3]成都中医药大学,四川成都610036

出　　处：《华西药学杂志》2002年第4期261-263,共3页West China Journal of Pharmaceutical Sciences

摘　　要：目的　建立藏药如意珍宝丸的鉴别和含量测定方法。方法　采用薄层色谱法和高效液相色谱法。结果　如意珍宝丸中 ,在荜茇、红花、肉桂、黄葵子、丁香和决明子等药材与对照药材相应的色谱位置处各有相同的斑点 ;并采用HPLC法测定了制剂中诃子的有效成份没食子酸的含量 ,其回归方程为A =6× 10 5C +718 14 (r =0 9998) ,RSD =1 5 8%。结论　所建立的鉴别与含量测定方法简便、准确 ,可用于如意珍宝丸的质量控制。OBJECTIVE To establish the TLC identification and quantitative determination methods for Ruyi Zhenbao pills.METHODS TLC and HPLC were adopted.RESULTS Rhizome Alpinia Officinarum,Abelmoschus Moschatus Medic,Semen Cassiae,Piper Longum,Flos Carthami,Flos Carthami and Flos Caryophylli were identified by TLC,and gallic acid in Ruyi Zhenbao pill was determined by HPLC. A =6×10 5 C +718.14( r =0.9998). RSD =1.56%,and average recovery was 97.34%.CONCLUSION These methods are simple and credible,and can be used to control the quality of Ruyi Zhenbao pill.

关 键 词：含量测定 薄层色谱法 高效液相色谱法 没食子酸 如意珍宝丸 药材鉴别 

分 类 号：R286.0[医药卫生—中药学]