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机构地区:[1]北京工业大学材料科学与工程学院,北京100124
出 处:《中国钨业》2017年第3期59-64,共6页China Tungsten Industry
基 金:国家自然科学基金创新研究群体项目(51621003)
摘 要:采用E3、Er-W、La-W1和La-W2四种材料作为氙灯的阴极材料,研究氙灯点灯一段时间后阴极的烧蚀形貌,分析阴极的烧蚀特征。结果表明:在电压3 000 V,频率3 Hz,电容23μF的条件下点灯100万发次,Er-W氙灯发黑最为严重,La-W2氙灯发黑程度最轻,管壁黑色物质是由阴极发生溅射形成的,成分由大量的WO3和少量的W组成;烧损后阴极端面的微观组织显示,Er-W阴极端面烧蚀凹坑最大,La-W2阴极的烧蚀坑最小,说明Er-W阴极工作温度较高,喷溅损失的材料较多,La-W2阴极的工作温度较低,材料的稳定性较好,从侧面说明La-W2的电子发射性能好;烧损后阴极纵截面金相组织显示,Er-W再结晶晶粒粗大,La-W2再结晶晶粒细小,细小的晶粒为第二相的扩散提供了更多通道,减轻材料的烧蚀。因此,Er-W阴极的抗烧损性能较差,La-W2阴极的抗烧损性能较好。This paper uses four kinds of materials (E3, Er-W, La-W1 and La-W2) as cathode materials of xenon lamp. Ablation morphology of xenon lamp cathode after lighting a period of time is studied. Ablation characteristics of cathode is analyzed. The results show that blackening degree of Er-W xenon lamp is most serious and blackening degree of Er-W xenon lamp is lightest under the condition of 3 0 0 0 V, 3Hz and 23 μF after lighting one million times. Black substance is formed by the cathode sputtering and the composition is composed of a large amount of W03 and a small amount of W. The microstructure of the cathode surface after ablation shows that the ablation pits size of the Er-W cathode is largest and the ablation pits size of the La-W2 cathode is smallest. This shows that the working temperature of Er-W cathode is higher and the working temperature of La-W2 cathode is lower. The electron emission property of La-W2 cathode is good. The microstructure of the cathode longitudinal section after ablation shows that the recrystallization grain size of Er-W cathode is large and the recrystallization grain size of La- W2 cathode is small. Fine grains provide more channels for the diffusion of the second phase and reduce the ablation of the material. Therefore, the anti ablation property of Er-W cathode is poor and the anti ablation property of La- W2 cathode is better.
分 类 号:TG146.411[一般工业技术—材料科学与工程] TM923.323[金属学及工艺—金属材料]
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