离子液体超声辅助提取磷脂酰肌醇  

Extraction of phosphatidylinositol by ionic liquid and ultrasonic wave method

作　　者：宋范范 张康逸 杨妍 杨帆 

机构地区：[1]河南省农业科学院,农副产品加工研究中心,河南郑州450002

出　　处：《食品工业科技》2017年第18期155-159,共5页Science and Technology of Food Industry

基　　金：河南省农业科学院科研发展专项资金项目(YCY20167822);河南省科技开放合作项目(152106000054)

摘　　要：以大豆粉末磷脂为原料,采用离子液体超声波辅助萃取的方法对磷脂酰肌醇进行了分离提取研究。考察了不同萃取次数、料液比、乙醇-离子液体(氢氧化1-丁基-3-甲基咪唑,[Bmim]OH)溶剂比、萃取温度、萃取时间和萃取功率对磷脂酰肌醇纯度和提取率的影响。结果表明:萃取次数3次,料液比1∶12(w/v),溶剂乙醇-[Bmim]OH体积比100∶7(v/v),萃取温度35℃,萃取时间15 min,萃取功率360 W条件下磷脂酰肌醇的纯度为79.53%±3.26%,提取率为68.26%±1.15%。The extraction methods of phosphatidylinositol from soybean lecithin powder by ionic liquid and ultrasonic wave were studied.The effects of extraction times,solid-liquid ratio,ehanol-[Bmim]OH ratio,extraction temperature,extraction time and ultrasonic power on the purity and extraction ratio of phosphatidylinositol were investigated. The purified phosphatidylinositol products were obtained at the conditions as follows： extraction times 3,solid-liquid ratio 1 ∶ 12,ehanol-[Bmim]OH ratio100∶ 7,extraction temperature 35 ℃,extraction time 15 min and ultrasonic power 360 W.Under these conditions,the purity and extracting yield of phosphatidylinositol were 79.53% ± 3.26% and 68.26% ± 1.15%,respectively.

关 键 词：大豆粉末磷脂 磷脂酰肌醇 超声波辅助萃取 离子液体 

分 类 号：TS229[轻工技术与工程—粮食、油脂及植物蛋白工程]