顶空气相色谱-质谱联用分析橡胶硫化烟气成分来源  

Component Source Analysis of Rubber Vulcanization Fume by HS-GC/MS

作　　者：吴爱芹 刘雪姣 温劭 王超 张清智 WU Aiqin;LIU Xuejiao;WEN Shao;WANG Chao;ZHANG Qingzhi(EVE Rubber Institute Co.,Ltd,Qingdao 266045,China)

机构地区：[1]怡维怡橡胶研究院有限公司,山东青岛266045

出　　处：《橡胶工业》2020年第3期225-229,共5页China Rubber Industry

摘　　要：建立顶空气相色谱-质谱(HS-GC/MS)联用分析橡胶(制品)硫化烟气成分的方法。对选定配方原材料及其混炼胶在硫化温度下挥发的烟气成分进行HS-GC/MS测试,确定挥发分成分;通过对定性结果的分析对比,推断硫化烟气各成分的来源。该方法的建立对开发绿色橡胶制品有很好的参考性。The method of analyzing the components of rubber(products)vulcanization fume by headspace gas chromatography-mass spectrometry(HS-GC/MS)was established.The fume components volatilized from raw materials and the compound of the formula under curing temperature were tested by HSGC/MS,and then the composition of volatiles were determined.According to the analysis and comparison of the qualitative results,the component source of the vulcanization fume was determined.This method could provide a good reference for the development of green rubber products.

关 键 词：橡胶 硫化烟气 挥发分 来源 顶空气相色谱-质谱 

分 类 号：TQ330.72[化学工程—橡胶工业] O657.63[理学—分析化学]