固相萃取技术在磺胺类药物残留分析中的研究进展  

Advances on Application of Solid Phase Extraction in Analysis of Sulfonamides Residues

作　　者：张艳梅 钱珊珊 赵志勇[1,2] 鄂恒超 范婷婷 李晓贝[1,2] 陈磊 董慧[1,2] 周昌艳 赵晓燕[1,2] ZHANG Yan-mei;QIAN Shan-shan;ZHAO Zhi-yong;E Heng-chao;FAN Ting-ting;LI Xiao-bei;CHEN Lei;DONG Hui;ZHOU Chang-yan;ZHAO Xiao-yan(Institute for Agri-food Standards and Testing Technology,Shanghai Academy of Agricultural Sciences,Shanghai201403,China;Laboratory of Quality and Safety Risk Assessment for Agri-food(Shanghai),Ministry of Agriculture and Rural Affairs,Shanghai201403,China;State Key Laboratory of Bioorganic and Natural Products Chemistry,Shanghai Institute of Organic Chemistry,Chinese Academy of Sciences,Shanghai200032,China)

机构地区：[1]上海市农业科学院农产品质量标准与检测技术研究所,上海201403 [2]农业农村部农产品质量安全风险评估实验室(上海),上海201403 [3]中国科学院上海有机化学研究所生命有机化学国家重点实验室,上海200032

出　　处：《分析测试学报》2020年第5期681-687,共7页Journal of Instrumental Analysis

基　　金：上海市市级农口系统青年人才成长计划资助项目(沪农青字(2018)第1-35号)。

摘　　要：磺胺类药物(Sulfonamides,SAs)残留与食品安全水平息息相关。存在SAs残留的基质复杂多样,开发快速、高效、高选择性的前处理方法是检测的关键。固相萃取(SPE)具有较少的溶剂使用量、绿色环保、高选择性、高灵敏度、节省时间、成本低、能与不同检测手段兼容等特点,已被广泛应用于SAs残留的前处理过程。该文简要介绍了移液枪头式SPE、磁性SPE、分子印迹SPE、管内SPE和其他SPE模式,并总结了它们在SAs残留检测分析中的研究进展。Sulfonamides(SAs)residues are closely related to food safety level.Development of rapid,efficient and highly selective pretreatment methods is the key point for determination of SAs owing to the presence of complicated matrices.Solid phase extraction(SPE),featuring with low solvent consumption,environmental friendliness,high selectivity,high sensitivity,timesaving,low cost and compatibility with different detection methods,has been widely applied in the sample pretreatment for SAs.In this review,advances of SPE application in the analysis of SAs are summarized,mainly including pipette tip SPE,magnetic SPE,molecularly imprinted SPE,in-tube SPE and other SPE.

关 键 词：固相萃取 磺胺类药物 残留分析 综述 

分 类 号：O657.7[理学—分析化学] R978.2[理学—化学]