改性羧甲基淀粉胶黏剂的制备及性能测试  

Preparation and characterization of modified carboxymethyl starch adhesive

作　　者：王小荣[1] 马国艳 惠瑞敏 WANG Xiao-rong;MA Guo-yan;HUI Rui-min(College of Chemistry and Chemical Engineering,Xianyang Normal University,Xianyang 712000,China;College of Chemistry and Chemical Engineering,Xi'an Shiyou University,Xi'an 710065,China)

机构地区：[1]咸阳师范学院化学与化工学院,陕西咸阳712000 [2]西安石油大学化学化工学院,陕西西安710065

出　　处：《化学工程师》2021年第5期11-13,共3页Chemical Engineer

基　　金：陕西省教育厅科研计划项目(19JK0926);咸阳师范学院青年骨干教师项目(XSYGG201806);2019年咸阳市科学技术研究发展计划项目(2019k02-22);咸阳师范学院(省级/校级)大学生创新创业训练计划资助项目(S202010722056,DC2020056);咸阳师范学院专项科研项目(XSYK18004)。

摘　　要：本实验通过淀粉和氯乙酸醚化反应制得改性羧甲基淀粉,同时以此改性淀粉为主要成分,成功制备了改性淀粉胶黏剂。通过红外光谱测试了改性淀粉的结构,通过干燥时间、耐水性、剥离强度等测试,研究了不同络合剂用量对改性淀粉胶黏剂的性能的影响。红外光谱测试结果表明,成功制得了改性淀粉。当络合剂用量为8mL时,干燥时间较短为57min,耐水时间较长为416s,剥离强度最大为53.63N·mm^(-1)。Modified carboxymethyl starch was successfully prepared by using chloroacetic acid as modifier,then the modified starch adhesive was prepared by mixing the carrier paste and the main body paste.The infrared spectrum(FTIR)test were used to characterize the structure of the modified starch.Effect of different content of complexing agent on the drying time,water resistance and peel strength of modified starch adhesive were all discussed.The FTIR results showed that the modified starch was successfully obtained.When the amount of complexing agent was 8mL,the drying time shortened to 57min,the water resistance time increased to 416s,the peel strength increased to 53.63N·mm^(-1).

关 键 词：改性淀粉 耐水性 剥离强度 

分 类 号：TQ432.2[化学工程]