两种对称结构的芴类衍生物的合成方法研究  

Study on the Synthetic Methods of Two Symmetrical Structures of Fluorene Derivatives

作　　者：高雅男[1] Gao Yanan(Hebei Chemical&Pharmaceutical College,Shijiazhuang 050000,China)

机构地区：[1]河北化工医药职业技术学院,河北石家庄050000

出　　处：《云南化工》2021年第7期59-61,共3页Yunnan Chemical Technology

基　　金：河北省教育厅20217年高等学校科学技术研究青年基金项目《DSA电极处理制药废水研究》(QN2014141)。

摘　　要：报道了9,9-二(4-羟乙氧基苯基)芴及9,9-二(3-甲基-4-羟基苯基)芴的合成方法,采用正交分析法研究了反应温度,时间等因素对收率的影响,并讨论了合成过程中可能出现的副产物结构,最终得到了两种目标物的最优合成方案。The synthesis of 9,9-bis[4-( 2-hydroxyethoxy) phenyl]fluorene and 9,9-bis( 3-methyl-4-hydroxyphenyl) fluorene were reported. The effects of reaction temperature and time on the yield were studied by orthogonal analysis. The possible by-product structures in the synthesis process were discussed. Finally,the optimal scheme for the synthesis of the two target compounds was obtained.

关 键 词：9 9-二(4-羟乙氧基苯基)芴 9 9-二(3-甲基-4-羟基苯基)芴 合成 副产物 

分 类 号：TQ243.1[化学工程—有机化工]