基础有机化学实验教学中的操作细节——常压蒸馏教学实践经验谈  

Operation Details in Teaching Basic Organic Chemistry Experiments:Practical Technique of Atmospheric Distillation

作　　者：李芳 赵卫光[2] Fang Li;Weiguang Zhao(National Demonstration Center for Experimental Chemistry Education,College of Chemistry,Nankai University,Tianjin 300071,China;State Key Laboratory and Institute of Elemento-Organic Chemistry,College of Chemistry,Nankai University,Tianjin 300071,China.)

机构地区：[1]南开大学化学学院,化学国家级实验教学示范中心,天津300071 [2]南开大学化学学院,元素有机化学研究所,天津300071

出　　处：《大学化学》2023年第1期206-212,共7页University Chemistry

摘　　要：“致广大而尽精微”是成事之道。常压蒸馏是有机化学实验的基本操作。在文献的查询过程中发现,无论教材还是文章,对常压蒸馏的一些操作细节都没有进行深入的讨论。很多学生,包括部分教师对蒸馏操作的细节都存在误区。根据多年的有机合成实践经验,对从仪器的安装、使用方法到蒸馏操作全过程中的细节和常犯的错误进行详细的解析,与同行共同探讨,使学生快速掌握蒸馏操作技巧。The devil is in the details.Although atmospheric distillation is a basic purification technique in organic chemistry,a literature search on the subject revealed that many practical details of the process are not explained in depth,whether in textbooks or articles.As a result,many students and even some teachers harbor misconceptions about distillation techniques.Based on knowledge acquired from years of practical experience in organic synthesis,this paper presents these missing details as well as common mistakes encountered throughout the distillation process,from the setup and use of the lab equipment to the distillation itself.It is hoped that this paper will facilitate fruitful discussions with peers and help students master distillation in the lab.

关 键 词：常压蒸馏 基本操作 教学 

分 类 号：G64[文化科学—高等教育学] O6[文化科学—教育学]