动物源性食品中氟喹诺酮类药物残留检测前处理技术的比较研究  

Comparative Study on Pretreatment Techniques for the Detection of Fluoroquinolones Residues in Animal Derived Foods

作　　者：陆向梅 胡波 宫平 魏佩玲 许艳丽 LU Xiangmei;HU Bo;GONG Ping;WEI Peiling;XU Yanli(Institute of Animal Husbandry Quality Standards,Xinjiang Academy of Animal Science,Urumqi 830000,China)

机构地区：[1]新疆畜牧科学院畜牧业质量标准研究所,新疆乌鲁木齐830000

出　　处：《食品安全导刊》2023年第13期130-132,145,共4页China Food Safety Magazine

基　　金：自治区公益性科研院所基本科研业务经费资助项目(ky2022004);新疆畜产品质量安全重点实验室(XJXS1412);自治区重点实验室开放课题(2020D04018)。

摘　　要：本文梳理了动物源性食品中氟喹诺酮类兽药残留检测的研究,了解当前国内的各类先进样品前处理技术,主要从色谱和色谱质谱联用法的角度,总结并论述不同基质样品、液相提取及洗脱条件、净化方式等对方法性能参数的影响,旨在提高动物源性食品中兽药残留的检测分析的效率和准确性,为后期建立同时检测多种兽药残留药物方法提供参考。This article reviews the research on the detection of fluoroquinolones residues in animal derived foods,understands various advanced sample pretreatment technologies in China,and summarizes and discusses the effects of different matrix samples,liquid phase extraction and elution conditions,purification methods,and other factors on the performance parameters of the method,mainly from the perspective of chromatography and chromatography-mass spectrometry,in order to improve the efficiency and accuracy of the detection and analysis of veterinary drug residues in animal derived foods,to provide reference for the establishment of a method for the simultaneous detection of multiple veterinary drug residues in the future.

关 键 词：动物源性食品 氟喹诺酮 前处理技术 检测 

分 类 号：TS218[轻工技术与工程—粮食、油脂及植物蛋白工程] O657.63[轻工技术与工程—食品科学与工程]