微波消解-原子荧光光谱法测定乳制品中锡的方法研究  

Determination of Tin in Dairy Products by Microwave Digestion and Atomic Fluorescence Spectrometry

作　　者：张艳 李璐 董文君 王琳帆 陈瑜程 李钢锋 ZHANG Yan;LI Lu;DONG Wenjun;WANG Linfan;CHEN Yucheng;LI Gangfeng(Inspection and Testing Center of Fuping County(Shaanxi Province Goat Milk Product Quality Supervision and Inspection Center),Fuping 711700,China;Shaanxi Goat Milk Gothic Dairy Co.,Ltd.,Fuping 711700,China)

机构地区：[1]富平县检验检测中心(陕西省羊乳产品质量监督检验中心),陕西富平711700 [2]陕西羊奶哥特医乳业有限公司,陕西富平711700

出　　处：《现代食品》2023年第11期172-175,共4页Modern Food

基　　金：陕西省市场监管局科研项目(2020ky15);渭南市科技计划项目(2022ZDYFJH-47)。

摘　　要：本试验采用微波消解-原子荧光光谱法对乳制品中的锡进行测定。结果表明,锡在0~200 ng·mL^(-1)线性关系良好,线性方程为y=50.096x+147.451,相关系数R2=0.999461。检出限、定量限、精密度均低于国标方法要求。此方法灵敏度高、重复性好、回收率高,可用于日常监管中乳制品检验检测分析。In this experiment,microwave digestion and atomic fluorescence spectrometry were used to determine tin in dairy products.The results showed that the linear relationship of tin in the range of 0~200 ng·mL^(-1) was good,the linear equation was y=50.096x+147.451,and the correlation coefficient was R2=0.999461.The detection limit,quantification limit and precision were all lower than the national standard method.This method has high sensitivity,good repeatability and high recovery rate,which can be used for the analysis of dairy products in daily supervision.

关 键 词：微波消解 原子荧光光谱法 乳制品 锡 

分 类 号：O657.3[理学—分析化学]