绿衣枳壳指纹图谱的研究  

Studies on the Fingerprint of Fructus Ponciri Trifoliatae Immaturi

作　　者：潘馨[1] 

机构地区：[1]福建省药品检验所,福州350001

出　　处：《海峡药学》2003年第6期40-41,共2页Strait Pharmaceutical Journal

基　　金：福建省卫生厅科研项目 ( 2 0 0 2- 15 )

摘　　要：目的 　应用 GC对绿衣枳壳药材挥发油进行指纹图谱研究。方法　色谱条件 :HP-1石英毛细管柱 ( 3 0 m× 0 .3 2 mm,0 .2 5μm) ,柱温条件 :起始温度 110℃ ( 2 0 min) 4℃·min- 1 14 0℃ ( 7min) 7℃· min- 1 2 2 0℃ ( 10 min) ;分流进样 ,分流比 1∶ 60 ;进样口温度 2 80℃。结果 　指纹图谱对绿衣枳壳中各成分均有较好分离。 结论 　该方法简便 ,准确 ,重现性好 。OBJECTIVE A Fingerprint of Fructus Ponciri Trifoliatae Immaturi has heen studied by GC.METHODS Sapillary column HP-1(30×0 32mm,0 25μm)was used, Column temperature:110℃ (20min) 4℃·min -1 140℃ (7min) 7℃·min -1 220℃ (10min); Split injection; split ration 1∶60. Injector temperature 280℃.RESULTS According to the chromatographic condition, a good fingerprint of Fructus Ponciri Trifoliatae Immaturi has been described.CONCLUSION The methods is simple, accurate with good reproducibility. It may be practical value for the quality control of sample for Fructus Ponciri Trifoliatae Immaturi.

关 键 词：仙茅 GC 指纹图谱 绿衣枳壳 挥发油 中药 

分 类 号：R284.1[医药卫生—中药学]