毛细管气相色谱法测定塑料食品包装袋中苯、乙酸乙酯的残留量  

DETERMINATION OF THE RESIDUAL BENZENE AND ETHYL ACETATE IN THE PLASTIC PACKING BAGS FOR FOOD BY CAPILLARY GAS CHROMATOGRAPHY

作　　者：梁振益[1] 邓广强[2] 罗盛旭[1] 杨雪蕊[1] 

机构地区：[1]海南大学理工学院,海口570228 [2]海南师范学院分析测试中心,海口571158

出　　处：《化学分析计量》2004年第1期40-41,共2页Chemical Analysis And Meterage

摘　　要：选用HP-FFAP型毛细管柱(30m×0.25mm i.d.,0.25 μm)和氢火焰离子化检测器,建立了测定塑料食品包装袋中苯、乙酸乙酯残留量的气相色谱分析方法。测定苯、乙酸乙酯的线性范围分别为0.120～4.000、0.170～4.000μg/mL,相关系数分别为0.9998、0.9995,检出限分别为0.048、0.068μg/mL,加标回收率分别为96.4％、100.8％,测定结果的相对标准偏差分别为3.1％、1.0％。HP - FFAP column (30 m×0.25 mm i. d. ,0.25μm) and hydrogen flame ionization detector were selected, a method for the determination of the organic residues namely benzene, ethyl acetate in the plastic packing bags for food was set up by capillary gas chromatography. The linear ranges for benzene and ethyl acetate are 0. 120 -4.000μg/mL and 0. 170 -4.000μg/mL, the correlative coefficients are 0.9998 and 0.9995, the detection limits are 0.048μg/mL and 0.068μg/mL respectively. The recovery and relative standard deviation of the method are 96.4% and 3. 1% for benzene and 100.8% and 1.0% for ethyl acetate respectively.

关 键 词：塑料食品包装袋 苯 乙酸乙酯 残留量 毛细管气相色谱法 

分 类 号：TS206.4[轻工技术与工程—食品科学] TS207.5[轻工技术与工程—食品科学与工程]