超临界CO_2从留兰香油中萃取香芹酮  

Extraction of Carvone from Spearmint Essential Oil By Supercritical CO_2

作　　者：罗运华[1] 刘以红[1] 

机构地区：[1]石油大学 (华东)重质油加工国家重点实验室

出　　处：《精细化工》2004年第2期119-120,128,共3页Fine Chemicals

摘　　要：用超临界CO2萃取法对留兰香毛油进行了萃取香芹酮的初步研究。工作是在实验室的小型装置上进行的。文中对实验装置和操作条件作了介绍。实验表明:在萃取塔底为50℃、塔顶为85℃,程序升压,使压力从8MPa升至13MPa时,可获得香芹酮质量分数为97%的馏分。Supercritical CO_2 extraction of carvone from spearmint essential oil was carried out in a laboratory mini installation.Experimental results showed that the extracted fraction containing 97% carvone could be obtained by setting the top temperature of extraction tower at 85 ℃ and the bottom temperature at 50 ℃ and rising the pressure gradually from 8 MPa to 11 MPa.The experimental installation and operating conditions were also discussed.

关 键 词：香料 留兰香油 超临界CO2 

分 类 号：TQ65[化学工程—精细化工]