supported by the National Natural Science Foundation of China(21073189,21006007,20901076,21176033);KnowledgeInnovation Program of DICP,Chinese Academic of Sciences(K2009D03)~~
Supported by the National Natural Science Foundation of China(Nos.20871051 and 20901076);the Scientific and Tech-nological Planning Project of Jilin Province, China(No.20080504)
A new tetradecaborate, [H3N(CH2)2NH3]2[B14O20(OH)6](1), was synthesized by a boric acid 'flux' method, and characterized by X-ray powder diffraction, ICP, IR, TGA and DTA analyses. Single-crystal X-ray diffrac...