Supported by National Natural Science Foundation of China (Grant Nos.20471041,20676086 and 20673072)
Nano-carbon materials were synthesized by the catalytic decomposition of acetylene at 400℃ by using Fe/Al2O3 as catalyst. The product was refluxed in 36% concentrated HCl at 60℃ for 48 h in order to re-move the cata...
Shanghai Municipal Education Commission (No. 05D215);Shanghai Sciences and Technologies Development Fund (No. 05JC14074);National Natural Science Foundation of China (No. 20673072);Shanghai Leading Academic Discipline Project (No. T0402)
The title compound N-(5,7-dimethoxy-2H-[1,2,4]thiadiazolo[2,3-a]pyrimidin-2- ylidene)-2-(2,4-dichlorophenoxy)propanamide 3 has been synthesized through using bromine as cyclic reagent in 66% isolated yield. Suitab...
Supported by Shanghai Municipal Education Commission (No. 05D215);Shanghai Sciences and Technologies Development Fund (No. 05JC14074) ;National Natural Science Foundation of China (No. 20673072)
The title compound N-(7-chloro-5-ethoxy-2H-[1,2,4]thiadiazolo[2,3-a]pyrimidin- 2-ylidene)- 2-(2,4-dichlorophenoxy)propanamide 3 has been synthesized through using bromine as cyclic reagent in 63% isolated yield. S...
Supported by Shanghai Municipal Education Commission (No. 05D215);Shanghai Sciences and Technologies Development Fund (No. 05JC14074); National Natural Science Foundation of China (No. 20673072) ;Shanghai Leading Academic Discipline Project (No. T0402)
Two novel chiral BINOL derivatives with bis(benzylamine) groups at the 3,3- positions have been synthesized through the condensation reaction between 2,2'-bis(methoxymethyleneoxy)-1,1'-binaphthyl-3,3'-dicarboxy...
Supported by the Shanghai Municipal Education Commission (No. 05D215);Shanghai Science and Technology Development Fund (No. 05JC14074);National Natural Science Foundation of China (No. 20543007 and 20673072)
The title compound (R)-3,3'-bis(benzyloxymethyl)-1,1'-bi-2,2'-naphthol (R)-3 has been synthesized through the deprotection of MOM group by iprOH/HCl in 83% isolated yield and the suitable single crystals for ...