financially supported by Key Laboratory of Hexi Corridor Resources Utilization of Gansu Universities(No.XZ1011 );the President's Funds of Hexi University(No.XZ-2009-9);the National Natural Science Foundation of China(No.21262010)
Received 20 November 2012 Received in revised form 13 December 2012 Accepted 21 December 2012 Available online 29 January 2013
A simple and efficient procedure for the preparation of silica-bonded propyl-diethylene-triamine-N-sulfamic acid (SPDTSA) by reaction of 3-diethylenetriamine-propylsilica (DTPS) and chlorosulfonic acid in chlorofo...
Boric acid (BO3H3) is an inexpensive, efficient and mild catalyst for the synthesis of 1,1-diacetate (acylal) from the various aromatic and heteroaryl aldehydes with acetic anhydride at room temperature under solv...
Ferrous methanesulfonate catalysing the conversion of aromatic, heteroaromatic, unsaturated, and aliphatic aldehydes to 1,1- diacetates at room temperature under solvent-free condition has been developed. The catalyti...
The partial support of this work by the University of Guilan Research Council is gratefully acknowledged.
Semicarbazones, 1,1-diacetates and acetals are efficiently converted to their corresponding carbonyl compounds using synergistic effect between KBrO3 and MoO3 in refluxing CH3CN-H2O in good to high yields.
Diacetates 1 and N-[(1-benzotriazol-l-yl)alkyl]amides 2, both masked forms of aldehydes, could undergo deprotection and condensation with cycloalkanones in a one-pot procedure promoted by samarium(III) iodide (SmI3) ...