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Synthesis,Characterization and Molecular Structure of a Diiron Complex(μ-SCH_2CH_2CH_2S-μ)Fe_2(CO)_5(Ph_2PCH_3)被引量：1
《Chinese Journal of Structural Chemistry》2016年第10期1563-1567,共5页刘旭锋 
Supported by the Natural Science Foundation of Zhejiang Province(No.LY16B020009);K.C.Wong Education Foundation
The title complex,（μ-pdt）Fe_2（CO）_5（Ph_2PCH_3）（pdt = SCH_2CH_2CH_2S）,was obtained by the reaction of the parent complex（μ-pdt）Fe_2（CO）_6 with Ph_2PCH_3 and Me_3NO·2H_2O in good yield（90%）. The title c...
关键词：diiron propanedithiolate monophosphine ligand carbonyl substitution synthesis crystal structure 
Synthesis and Crystal Structure of the Diiron Azadithiolate Complex [(μ-SCH_2)_2NPh]Fe_2(CO)5(Ph_2PCH_2PPh_2)被引量：5
《Chinese Journal of Structural Chemistry》2011年第10期1437-1441,共5页刘旭锋 肖勋文 刘幸海 
supported by the National Natural Science Foundation of China (20902051,21002090);the Key Laboratory of Pesticide Chemistry and Application,Ministry of Agriculture (MOA) (No.MOAPCA201005);the Foundation of the Education Committee of Zhejiang Province (Y201018479,Z200906833);the Natural Science Foundation of Ningbo (2010A610186)
Reaction of [（μ-SCH2）2NPh]Fe2（CO）6 with Ph2PCH2PPh2 in the presence of Me3NO·2H2O gave the title complex [（μ-SCH2）2NPh]Fe2（CO）5（Ph2PCH2PPh2）（1）in 78% yield.The new complex 1 was characterized by element...
关键词：diiron azadithiolate SYNTHESIS crystal structure 
Synthesis,Characterization and Crystal Structure of a Diiron Azadithiolate Complex [(μ-SCH_2)_2NCH_2Ph]Fe_2(CO)_5(PPh_3)
《Chinese Journal of Structural Chemistry》2011年第7期1016-1020,共5页刘旭锋 肖勋文 沈梁钧 房江华 王家荣 高浩其 刘幸海 
Supported by the start-up foundation of Ningbo University of Technology;the National Natural Science Foundation of China (20902051,21002090);Foundation of the Education Committee of Zhejiang Province (Z200906833);the Natural Science Foundation of Ningbo city (2010A610186)
Treatment of complex [（μ-SCH2）2NCH2Ph]Fe2（CO）6 with PPh3 in the presence of decarbonylating agent Me3NO-2H2O afforded the rifle complex [（μ-SCH2）2NCH2Ph]Fe2（CO）5（PPh3） in 70% yield. The new complex was cha...
关键词：diiron azadithiolate PPH3 SYNTHESIS crystal structure 
Synthesis and Crystal Structure of a Model for the Active Sites of Fe-only Hydrogenases:[Fe_2(SCH_2)_2N(3-PhCF_3)(CO)_6]_2
《Chinese Journal of Structural Chemistry》2007年第1期113-117,共5页程岚霞 马成丙 胡明强 陈昌能 刘秋田 
This project was supported by the NNSFC (No. 20471061) and the Science & Technology Innovation Foundation for the Young Scholar of Fujian Province (No. 2005J059)
A model compound for the active sites of Fe-only hydrogenases, [Fe2（SCH2）2N（3- PhCF3）（CO）6]2, has been synthesized and structurally characterized by single-crystal X-ray diffraction. It crystallizes in tetragona...
关键词：Fe-only hydrogenases crystal structure iroa-suifur duster 
Structures that should be Described in Higher-Symmetry, Centrosymmetric Space Groups. Part 1. The Disordered Structures of [(CH_3CH_2)_4N]_3{[(SCH_2CH_2S)MoS_3]_2Fe}, [(CH_3CH_2)_4N]_2{[S_2CN(C_2H_5)_2]_4Fe_4S_4} and [(CH_3CH_2)_4N]_3{[(SCH_2C
《Chinese Journal of Structural Chemistry》2000年第6期405-410,共6页
关键词：SCH2CH2S)MoS3 CH3CH2 C2H5 S2CN Structures of Fe 
Synthesis,Structure,Characterization and Electrochemistry of a New Dinuclear W(0)-complex〔Et_(4)N〕_(2)〔W_(2)(CO)_(8)(SCH_(2)COOMe)_(2)〕
《Chinese Journal of Structural Chemistry》1999年第1期34-39,共页
Reaction of Et 4NCl, NaSCH 2COOMe and W(CO) 6 in MeCN affords a new dinuclear tungsten(0) complex Et 4N 2 W 2(CO) 8(SCH 2COOMe) 2 (1). The crystal and molecular structure has been determined by X ray ...
关键词：tungsten(0) complex STRUCTURE IR spectra 13  C NMR and electrochemistry 
STRUCTURE OF [Et_4N]_2[Mo_2(CO)_8(SCH_2C_6H_4CH_2SH)]
《Chinese Journal of Structural Chemistry》1989年第1期19-22,共4页黄梁仁 庄伯涛 等 
Mr =1015.05, P21/c, a= 10.912(4), b= 12.088(3), c= 18.807(8) A.β=103.57(3)° ,V= 2411.4 A3, Z = 2, DC = 1.40 g/cm3.λ(MoKα)= 0.71073 A, μ=7.2 cm-1,F(000)=1048.Room temperature, final R=0.069, Rw=0.091. The geometry...
关键词：四乙基铵 羰基 二元配合物 钼 晶体结构 邻苯二甲硫醇 
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