动物及动物源性食品中六氯苯、六六六和滴滴涕微量化气相色谱法快速检测  

Determination of HCB,BHC and DDt residues in the animal & animal product by gas chro-matography with microvolumelization extraction

作　　者：吴雅红[1] 张思群[2] 

机构地区：[1]广东工业大学轻化学院食品教研室,广东广州510090 [2]广州出入境检验检疫局食品实验室,广东广州510623

出　　处：《佛山科学技术学院学报（自然科学版）》2004年第4期70-73,共4页Journal of Foshan University(Natural Science Edition)

摘　　要：采用微量化提取,并结合毛细管柱气相色谱法测定动物及动物源性食品中六氯苯、六六六和滴滴涕的残留。结果表明,该方法简便、快速,可同时连续检测大量样品。且此方法平均回收率在86.15%～102.9%之间,相对标准偏差在2.0%～10.9%之间,结果准确、可靠。同时得出本方法HCB,BHC(总)及DDT(总)测定的低限。This paper deals with the determination of HCB,BHC and DDT residues in the animal & animal product by capillary gas chromatography with microvolumelization extraction. It shows that the method is simple and convenient in continuous determining a large quantity of samples at the same time with the average recoveries at 86.15%～102.9% and the RSD in the range of 2.0%～(10.9%).The result is exact and reliable The detection limits are 0.002 mg/kg(HCB),0.04 mg/kg(BHC),0.04 mg/kg(DDT).

关 键 词：微量化 动物及动物源性食品 六氯苯 六六六 滴滴涕 气相色谱 

分 类 号：TS207.53[轻工技术与工程—食品科学]