二盐酸双咪苯脲结构解析与含量测定方法的研究  

Study on the structure and method for the content detection of imidocarb dihydrochloride

作　　者：畅丽芳[1] 戴国华 杨永嘉[3] 

机构地区：[1]吉林大学五星动物保健有限公司,吉林长春130062 [2]军科院兽医研究所,吉林长春130062 [3]中国兽医药品监察所,北京100081

出　　处：《中国兽药杂志》2005年第12期28-31,共4页Chinese Journal of Veterinary Drug

摘　　要：采用元素分析、IR、UV、MS和NMR方法测定了二盐酸双咪苯脲的化学结构并进行解析,同时建立了二盐酸双咪苯脲的UV含量检测方法。结果,波谱和元素分析等确证了二盐酸双咪苯脲的化学结构。用UV法测定其水溶液含量时,浓度与吸收度呈良好的线性关系,重现性和稳定性都较好。A method for determination of imidocarb dihydrochloride was presented. The structure was proved by IR, UV, MS, ^1H-NMR, ^13C-NMR and elementary analysis. The content was determined by spectrophotometry. The results showed that there was a good linear relationship between the concentration of IMD and the absorbance with good reproducibility and stability.

关 键 词：二盐酸双咪苯脲 分光光度法 质谱 核磁共振 化学结构 UV含量检测方法 重现性 稳定性 

分 类 号：S859.2[农业科学—临床兽医学]