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作 者:黄亚非[1] 张永明[1] 黄际薇[1] 李瑞珍[1] 刘杰[1]
出 处:《中国中药杂志》2006年第11期898-900,共3页China Journal of Chinese Materia Medica
摘 要:目的:研究黄皮果药材中挥发油和微量元素的组成及含量。方法:采用二氧化碳超临界法萃取挥发油,用HP6890GC-5973MS进行分析,归一法测定其相对含量,并用GC-MS鉴定化学成分。利用SPECTRO CIROS等离子体原子发射光谱仪、Agilent 7500a型电感耦合等离子体发射质谱仪和915-塞曼测汞仪直接进行测定微量元素。结果:共鉴定出36个挥发油成分,占挥发油总组分的95%以上;并测定出11种微量元素。结论:首次从该植物中鉴定出18种挥发油成分。Objective: To study and determine the chemical constituents of the volatile oil and the trace elements in the fruits of the Clausena lansium. Method: The essential oils were extracted by supercritical fluid extraction (SFE) and separated on capillary columns with HP6890GC-5973MS. The components were quantitatively determined with nomalization method, and were identified with GC-MS. And the trace elements were determined by ICP-MS and ICP-AES. Result: 36 Components constituting 95% of the total essential oil were separated and identified, and 11 trace dements were identified. Conclusion: 18 Compounds were found from the fruit of C.lansium for the first time.
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