山楂果实中黄酮类化合物的超高压提取研究  被引量:3

Extract Flavonoids of Hawthorn by Ultrahigh Pressure

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作  者:骆晓沛[1] 张守勤[1] 张格[1] 曹金钰[1] 闫洪森[2] 

机构地区:[1]吉林大学生物与农业工程学院,长春130022 [2]长春大学电子信息工程学院,长春130022

出  处:《农机化研究》2008年第7期168-171,共4页Journal of Agricultural Mechanization Research

摘  要:用常温超高压技术提取山楂中黄酮类化合物,为了研究提取的最佳工艺,采用正交试验优化,利用分光光度法检测提取液中总黄酮含量。结果表明,超高压提取山楂果中黄酮类化合物的最佳提取工艺参数分别为:提取溶剂为50%乙醇,料液比为1:40,浸泡时间2h,提取压力300MPa,提取时间为3min。超高压提取时间短,提取液澄清稳定。The ultrahigh pressure extraction method was used to extract flavonoids from Hawthorn at normal temperature. The content of flavonoids was determined by UV - spectrophotometry. Parameters that may influence the extraction process were investigated. The orthogonal test was applied to obtain the optimum extraction condition, which was as follows : solvent of 50% ethanol, ratio of raw Hawthorn (g) to solvent (mL) of 1:40, marinate time of 2 hours, extraction pressure of 300mPa and extraction time of 3 min. Results of this work show that the ultrahigh pressure extraction method has several advantages, such as shorter extraction time, and less impurity in the extracted flavonoids.

关 键 词:山楂果 黄酮类化合物 超高压提取 正交设计 

分 类 号:TQ914.1[化学工程] R284.2[医药卫生—中药学]

 

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