玉米中阿特拉津残留量的测定方法研究  

Residual Determination Method of Atrazine in Corn

作　　者：毛应明[1] 王学松[1] 朱平华[1] 张成燕[1] 熊建军[1] 

机构地区：[1]淮海工学院化学工程学院,江苏连云港222005

出　　处：《食品科学》2008年第7期336-339,共4页Food Science

基　　金：江苏省应用化学重点学科项目(BK2005045);淮海工学院自然科学基金项目(KK04030)

摘　　要：通过综合运用微波萃取、柱层析和气相色谱氮磷检测器法分析研究玉米中阿特拉津残留量的测定方法。该方法的加标回收率为92%～104%,相对标准偏差(RSD)为1.47%～4.35%,样品中的检出限为0.0005mg/kg。与国家标准(GB/T5009.132-2003)中的测定方法相比,本方法的样品提取时间大大缩短,试剂用量减少,精密度和准确度都有所提高。Microwave-assisted extraction, integrated with column chromatography and gas chromatography with a nitrogen-phosphorus detector, was presented for residual determination of atrazine in corn. The recoveries of the method range from 92% to 104%. The relative standard deviation is between 1.47% and 4.35%. Compared with the method in China National Standards （GB/T 5009.132-2003）, this is a rapid method with less solvent consumption and better precision and accuracy.

关 键 词：玉米 阿特拉津 测定方法 微波萃取技术 

分 类 号：TS207.53[轻工技术与工程—食品科学]