SBSE-TDS-GC-MS测定烟草表香挥发性与半挥发性成分  

Analysis of volatile and semi-volatile ingredients in tobacco spices using SBSE-TDS-GC-MS

作　　者：刘汗青[1,2] 金诚[1] 杨新周[1] 曾程[1] 杨叶昆[2] 戴云[1] 

机构地区：[1]云南民族大学化学与生物技术学院,云南昆明650500 [2]云南烟草科学研究院香精香料室,云南昆明650106

出　　处：《化学试剂》2011年第8期723-726,共4页Chemical Reagents

摘　　要：以固态萃取搅拌棒为样品前处理技术,采用气相色谱/质谱联用法分析了烟草表香挥发性与半挥发性成分。对影响萃取效果的实验条件进行了考察,并采用正交实验法对影响热解吸的3个主要实验参数(热解吸温度、解吸时间和进样口冷聚焦温度)进行考察,得到优化的实验条件。结果表明,同一样品经6次测定,所得27个组分峰面积的相对标准偏差(RSD)平均值小于10%,实验证明该方法具有较高的准确度和较好的重现性,可用于烟草表香的快速分析测定,也可成为烟用香精香料质量控制的有效手段。The voliate and semi-voliate ingredients of tobacco spices was analysized using stir bar sorptive extraction coupled to gas chromatography-mass spectrometry. The experimental conditions affecting extraction effect was optimized, and three main factors affecting thermal desorption（ desorption temperature, desorption time, cold hydrazine temperature） was also investigated by the method of orthogonal test. The average relative standard deviation（RSD） of peak areas of 27 components for 6 determinations was less than 10%. Therelore,this method can satisfy the requirements for the rapid analysis of tobacco spices and be also used to control the quality of tobacco flavor.

关 键 词：烟草表香 固态萃取搅拌棒 热解吸 气相色谱-质谱 

分 类 号：TQ651[化学工程—精细化工]