金银忍冬果实中挥发性成分的GC-MS分析  

Volatile Constituents of Lonicera macckii Fruit by GC-MS

作　　者：姬晓灵[1] 雍建平[1] 汪岭[1] 

机构地区：[1]宁夏医科大学公共卫生学院

出　　处：《光谱实验室》2011年第6期3110-3112,共3页Chinese Journal of Spectroscopy Laboratory

基　　金：宁夏自然科学基金(NZ10108);宁夏医科大学面上基金(XM201010);宁夏医科大学博士建设开放课题(KF2010-12)

摘　　要：研究宁夏生长的金银忍冬果实中挥发性物质的化学成分。用乙醚作溶剂,采用索氏提取法从宁夏生长的金银忍冬果实中提取挥发性物质,并通过GC-M S联用技术对挥发性成分进行了分析鉴定,用色谱峰面积归一化法计算了各成分的相对含量。从宁夏生长的金银忍冬果实中提取的挥发性物质中鉴定了32种化合物,其中含量最大的是甲基己基过氧化氢(1.31%);化合物洋地黄毒苷,9-[2′,2′-二甲基丙酰腙]3,6二-氯-2,7双-[2-[二乙氨基]乙氧基]芴和胆甾-22-烯-21醇-,3,5脱-氢-6-甲氧基特戊酸酯为具有复杂结构的化合物。The volatile constituents from the Lonicera macckii fruit that planted in Ningxia were studied.The volatile constituents were obtained by soxhlet extraction method with ether as solvent,and that analyzed by GC-MS.And relative content of each component was determined by peak area normalization.32 compounds were identified.Methyhexyl-hydroperoxide was the major constituent（1.31%）,and compouds of digitoxin,9-[2′,2′-dimethylpropanoilhydrazono]-3,6-dichloro-2,7-bis-[2-[diethylamino]-ethoxy]fluorene and cholest-22-ene-21-ol,3,5-dehydro-6-methoxy-pivalate had the complex structure.

关 键 词：金银忍冬 果实 挥发性成分 气相色谱-质谱 

分 类 号：O657.63[理学—分析化学] O657.71[理学—化学]