肉苁蓉中苯乙醇糖苷提取及在卷烟中的应用研究  

Extraction of Phenylethanoid Glucosides in Cistanches salsa Beck and It Application in Cigarette

作　　者：赵秋蓉 吴迪 祖萌萌[2] 纪旭东 张峻松[2] 

机构地区：[1]内蒙古昆明卷烟有限责任公司,内蒙古呼和浩特010020 [2]郑州轻工业学院食品与生物工程学院

出　　处：《安徽农学通报》2012年第10期38-39,64,共3页Anhui Agricultural Science Bulletin

摘　　要：考察了乙醇浓度、提取时间、提取温度对肉苁蓉提取量的影响。实验结果表明:肉苁蓉提取量随着乙醇浓度的升高先是逐渐升高然后又呈现下降的趋势;当乙醇浓度和提取温度一定时,肉苁蓉提取得率随提取时间的延长而增加,当固定肉苁蓉的提取时间和提取用乙醇的浓度,肉苁蓉提取随着提取温度的增加,通过实验表明肉苁蓉提取条件为:乙醇浓度为70%,提取时间为4h,提取温度为70℃。以V(乙酸乙酯):V(甲醇)=15:1的混合溶剂为洗脱剂,用柱层析法分离得到苯乙醇糖苷。通过卷烟加香试验发现,肉苁蓉苯乙醇糖苷能有效地掩盖卷烟杂气,使烟气柔和、余味舒适、回甜感好、香气细腻,对改进烟气质量作用明显。The affluence of alcohol concentration, extraction time and extraction temperature on the yield of the Cistanches salsa Beck were investigated. The yield of the Cistanches salsa Beck increased with the concentration of alcohol increasing at first, and then decreased as the alcohol concentration keep on increasing. The yield also increased with the extraction time when the alcohol concentration and extraction h temperature were fixed. As the alcohol concentration and extraction time were 4h. The optimum technology of extracting Cistanches salsa Beck was as follows： The extraction time is 4h, the extraction temperature is 70℃ and the alcohol concentration is 70%. The phenylethanoid glucosides in Cistanches salsa Beck were separated with column chromatography, and use V （ ethyl acetate ） ：V （ methyl alcohol ） =15：1 for eluent. The phenylethanoid glucosides of Cistanches salsa Beck was applied in cigarettes as tobacco flavorant. The results indicated that it could efficiently reduce offensive odor, make tobacco smoke smooth and fine, and improve smoking quality of the cigarettes.

关 键 词：肉苁蓉 提取 苯乙醇糖苷 卷烟 感官评价 

分 类 号：O949.778.3[理学]