顶空固相微萃取-气质色谱联用技术分析海州香薷与石香薷中挥发性成分  被引量:8

Analysis of Volatile Chemical Constituents from Two Species of Elsholtzia Herb by HS-SPME-GC-MS

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作  者:李佳[1] 刘红燕[1] 张永清[1] 

机构地区:[1]山东中医药大学山东省高校中药资源学重点实验室,济南250355

出  处:《中国实验方剂学杂志》2013年第16期118-122,共5页Chinese Journal of Experimental Traditional Medical Formulae

基  金:国家"重大新药创制"科技重大专项(2010ZX09401-302-5-12)

摘  要:目的:对石香薷和海州香薷中挥发性化学成分进行研究。方法:采用顶空固相微萃取-气相质谱联用技术对2种香薷植物挥发性成分进行提取分离和鉴定研究。结果:从海州香薷和石香薷挥发性成分中分别检出39,46种成分,分别占挥发性成分总峰面积的70.50%,92.44%。结论:香薷挥发性成分中主要含高级烷烃、烯烃、醇、酮、酚及有机酸等多种化学成分,具有较高的医药、食品应用价值,为香薷资源的进一步开发利用提供了科学依据。Objective: To study the volatiles from Elsholtzia splendens and Molsa chinese. Method: The volatile chemical constituents from E. splendens and M. chinensis, were analysed by HS-SPME-GC-MS. Result:Thirty-nine and forty-six components from E. splendens and M. chinese, which accounted for 70. 55% and 92.44% of the peak areas, were separated and identified. Conclusion: The volatile chemical constituents have high application value in medicine and chemical industry and mainly consisted of alkane, olefin, alcohol, ketone, phenol, organic acid, etc. The present experiments provide a scientific basis for the further exploitation and utilization of this herb.

关 键 词:顶空固相微萃取法 气相-质谱联用 香薷 挥发性成分 

分 类 号:R284.1[医药卫生—中药学]

 

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