烟叶中核心香气成分的GC/MS分析  

GC/MS Analysis of Kernel Flavor Ingredients in Tobacco Leaf

作　　者：李天飞[1] 孙敏[1] 杨金辉[1] 张承聪[2] 杨文凡[2] 杨艳[2] 马东萍 叶兰钦[1] 

机构地区：[1]云南烟草科学研究院,云南昆明650106 [2]云南大学化学系,云南昆明650091

出　　处：《云南大学学报（自然科学版）》2001年第3期217-221,共5页Journal of Yunnan University(Natural Sciences Edition)

摘　　要：采用索氏提取技术对烟叶末样品的挥发性成分进行提取 ,用GC/MS和双柱复检法对烟叶中的核心香气成分进行了定性 ,半定量分析 .质谱共鉴定了 6 5种香气成分 ,为定量分析奠定了基础 .由于在样品前处理中采用丙酮直接萃取核心香气成分 ,避免了传统的碱洗 ,酸洗过程 ,获得了比较客观的分析结果 ,为烟叶中核心香气成分的分析开拓了崭新的研究思路 .Soxhlet Extractor has been applied to extract volatile ingredients of tobacco leaf and Gas/Mass has also been used to identify the flavor ingredients in tobacco samples by double columns' check (apolar and polar).GC/MS identified 67 compounds with flavor in tobacco leaf and lay a foundation for quantitative analysis.During pretreatment,kernel flavor constituents are exacted by acetone directly,traditional alkali wash and acid wash steps were cancelled,and hence we obtain a much objective analysis result.This research opens up a new investigate way for analysis of kernel flavor ingredients in tobacco leaf.

关 键 词：烟叶 香气 气质联用 成分分析 色谱/质谱分析 GC/MS分析 双柱复检法 

分 类 号：TS411[农业科学—烟草工业]